MS Report File ..0150120 2015-01-20 09-25-28\\WGY2445-011-1.D Tgt Mass (CHM): Injection Date : 20 Jan 15 1:49 pm +0800 Seq. Line : 49 Sample Name : WGY2445-011-1 Location : Vial 44 Acq. Operator : Li Shan(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul Acq. Method : D:\\Aglient 1260\\Data\\20150120\\20150120 2015-01-20 09-25-28\\100-1000MS+3MIN( Analysis Method : D:\\Aglient 1260\\Method\\WASH-COL2-5MIN.M Catalog No : HY-13032 Batch#14774 A-RP-124 Method Info : DAD1 B, Sig=214,4 Ref=off 1.623mAU150010001.8561.9952.0961.3521.49700.5 DAD1 C, Sig=254,4 Ref=off mAU1500100050000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 506000004000001.2602.1762.29050011.5 A1r.e355a: 8.719 A1r.e50002a: 14.78 A73rea1.621: 5876.1622.53min A1.56r8ea: 50.27 A1.9633r9ea: A 482.09re6.37a A: 2222.770.r1ea3: 90 A11.12.8723r2ea99: 11.09221.51.61222.53min1.8271.9622.0701.3281.4742000002.1820.51 Ion 0, MSD1 0,Target Mass 0 Positive, EIC=-0.30:0.70 0.050-0.05-0.10.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.53min1.522.53min RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.35 0.06 16.33 4.94 0.23 1.50 0.05 19.00 7.03 0.26 1.62 0.05 6827.94 2302.44 94.90 1.86 0.05 113.54 38.42 1.58 1.99 0.06 115.49 34.53 1.61 2.10 0.04 60.58 23.79 0.84 2.18 0.04 11.35 4.78 0.16 2.29 0.05 30.49 10.90 0.42 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.35 0.05 8.72 2.81 0.14 1.50 0.05 14.79 4.62 0.24 1.62 0.05 5876.16 2135.07 97.27 1.86 0.05 50.27 17.12 0.83 2.00 0.04 48.37 19.10 0.80 2.10 0.05 20.39 7.46 0.34HY-LCMS-02 1/20/2015 2:45:57 PM Li Shan(LCMS-02)Page 1 of 4
MS Report 2.18 0.05 11.24 4.09 0.19 2.29 0.07 11.09 2.58 0.18HY-LCMS-02 1/20/2015 2:45:57 PM Li Shan(LCMS-02)Page 2 of 4
MS ReportRet. Time: 1.26 <<<< POSITIVE SPECTRA >>>> ES-API Positive 102.2Ret. Time: 1.33 ES-API Positive12000 102.21200010000100008000 199.0 197.08000 221.660006000 105.1 137.1 279.1 340.3 396.9 137.1 222.000 105.14000 453.4 103.2 153.0 153.0 200.00200400600800m/z 701.4 792.60200400600800m/zRet. Time: 1.47 ES-API Positive 102.2Ret. Time: 1.61 ES-API Positive 424.1120001000001000080000 390.28000 199.060000 425.1 426.1 102.2 212.6 427.16000 105.1 195.0000 221.6 391.14000 137.1 279.1 101.2 153.1 442.1 198.0 222.40200400600m/z0200400600800m/zRet. Time: 1.83 ES-API Positive 466.2Ret. Time: 1.96 ES-API Positive 367.216000140001200010000 105.1 233.6 102.217500 102.2150001250010000750080006000400020000 467.1 468.2 500.2 105.1 368.1 425.1 424.1 130.2 199.0 137.1 130.3 251.3 199.0 480.2 381.5 137.1 501.1 212.6 240.6 212.7 446.5500025000 481.1 446.1 279.0 279.1 360.7 103.1200400600800m/z 426.1 736.1 733.1 869.3200020000 197.92000 279.12000 443.1 442.1200400600800m/zHY-LCMS-02 1/20/2015 2:45:57 PM Li Shan(LCMS-02)Page 3 of 4
MS ReportRet. Time: 2.07 ES-API Positive 105 .102.2Ret. Time: 2.18 ES-API Positive 105.1 576.21400012000100008000175001500012500 130.2 288.710000 577.1 197.060004000 2.475005000 130.2 425.2 424.1 197.1 137.1 279.1 137.1 424.1 103.2 279.1 598.2 367.1 446.10200400600800m/z 182.20200400600m/zHY-LCMS-02 1/20/2015 2:45:57 PM Li Shan(LCMS-02)Page 4 of 4
588.22500 182.22000 552.7 101.2 301.1 552.8
